in dichloromethane under Ar; CH2Cl2 added to mixt. of Rh complex and Ph3CBF4, added acetonitrile; concd. in vac., pptd. by addn. of Et2O, filtered, washed with Et2O;
参考文献
Journal of the American Chemical Society, , vol. 105, # 25 p. 7288 - 7294
in benzene byproducts: Ph3C; under N2; (Ph3C)BF4 (1 equiv.) added to Re complex in benzene; reacted at ambient temp. for 24 h; detd. by UV-vis and mass spectra;
