Sammes, Michael P.; Leung, Christopher W. F.; Mak, Chi Keung; Katritzky, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1585 - 1590
in dichloromethane
under Ar, Ph3CBF4 and Fe complex mixed in solid state, at 0°C added CH2Cl2, kept for 100 h from -10 to 10°C; ppt. centrifuged, washed with hexane, dried at room temp. in vac.;
参考文献
Suenkel, Karlheinz; Nagel, Ulrich; Beck, Wolfgang
Journal of Organometallic Chemistry, 1983 , vol. 251, # 2 p. 227 - 244
hydrogen in tetrahydrofuran
T=-60 - 20°C; P=2250.23 Torr; Inert atmosphere;
参考文献
Runyon, Jason W.; Steinhof, Oliver; Dias, H. V. Rasika; Calabrese, Joseph C.; Marshall, William J.; Arduengo, Anthony J.
Australian Journal of Chemistry, 2011 , vol. 64, # 8 p. 1165 - 1172
