3-丁氧基-4-甲氧基苯甲醛合成路线 （共 7 条）
反应条件
potassium carbonate in N-methyl-acetamide
参考文献
Nikken Chemicals Co., Ltd.
Patent: US6265402 B1, 2001 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=110°C;
参考文献
Zhang, Mei; Yang, Xiao-Ying; Tang, Wei; Groeneveld, Tom W. L.; He, Pei-Lan; Zhu, Feng-Hua; Li, Jia; Lu, Wei; Blom, Anna M.; Zuo, Jian-Ping; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 4 p. 317 - 321
参考文献
American Home Products Corporation
Patent: US5124455 A1, 1992 ;
反应条件
1: potassium carbonate; potassium iodide / ethanol / 15 h / |Reflux 2: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice View Scheme
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
trichlorophosphate T=100 - 115°C; Vilsmeier-Haack Formylation; 19 h; Cooling with ice; Overall yield = 83.1 percent; Overall yield = 6.8 g;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
sodium chlorite; aminosulfonic acid; acetic acid
1 h; Ambient temperature;
参考文献
Zhang, Mei; Yang, Xiao-Ying; Tang, Wei; Groeneveld, Tom W. L.; He, Pei-Lan; Zhu, Feng-Hua; Li, Jia; Lu, Wei; Blom, Anna M.; Zuo, Jian-Ping; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 4 p. 317 - 321
