3-苯基-1,2,4-三唑-5-硫醇水合物合成路线 （共 27 条）
反应条件
1: 76 percent / sodium acetate / acetic acid / 2 h / Heating
2: 73 percent / acetic anhydride / Heating
3: 68 percent / hydrazine hydrate / ethanol / 0.5 h / Heating
View Scheme
参考文献
Ali, Mohamed I.; Soliman, Adly A.-W.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 869 - 875
反应条件
1: 76 percent / sodium acetate / acetic acid / 2 h / Heating
2: 73 percent / acetic anhydride / Heating
3: 70 percent / 1 h / Heating
View Scheme
参考文献
Ali, Mohamed I.; Soliman, Adly A.-W.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 869 - 875
反应条件
1: 84 percent / sodium acetate / acetic acid / 2 h / Heating
2: 82 percent / acetic anhydride / 1 h / Heating
3: 76 percent / 1 h / Heating
View Scheme
参考文献
Ali, Mohamed I.; Soliman, Adly A.-W.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 869 - 875
反应条件
1: aq. NaOH
2: 2N aq. NaOH / 1 h / Heating
View Scheme
参考文献
Simiti; Marie; Coman; et al.
Archiv der Pharmazie, 1987 , vol. 320, # 6 p. 528 - 534
反应条件
sodium acetate; acetic anhydride; acetic acid
Heating;
参考文献
Prasad, A. R.; Rao, A. Narasimha; Ramalingam, T.; Sattur, P. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 776 - 778
反应条件
sodium acetate; acetic anhydride in acetic acid
Cyclization; condensation; 6 h; Heating;
参考文献
Tozkoparan, Birsen; Kilcigil, Guelguen Ayhan; Ertan, Rahmiye; Ertan, Mevluet; Kelicen, Pelin; Demirdamar, Ruemeysa
Arzneimittel-Forschung/Drug Research, 1999 , vol. 49, # 12 p. 1006 - 1011
反应条件
sodium acetate; acetic anhydride in acetic acid
Cyclization; condensation; 6 h; Heating;
参考文献
Tozkoparan, Birsen; Kilcigil, Guelguen Ayhan; Ertan, Rahmiye; Ertan, Mevluet; Kelicen, Pelin; Demirdamar, Ruemeysa
Arzneimittel-Forschung/Drug Research, 1999 , vol. 49, # 12 p. 1006 - 1011
