反应条件
KBr; Br2 in ethylene glycol dimethyl ether malonitrile and potassium bromide dissolved in water, bromine added at 5°C to stirred soln., dibromomalonitrile-potassium bromide complex produced was removed by filtration, washed with water, dried over P2O5under high vac.; potassium cyanide dissolved in dimethoxyethane, potassium bromide complex added, stirred for 1.5 h, heated to reflux briefly, hot soln. filtered, cooled overnight, crystn. by adding ether, filtration;
参考文献
Inorganic Chemistry, , vol. 21, p. 581 - 586