4-氨基苯基-alpha-D-吡喃甘露糖苷合成路线 （共 6 条）
反应条件
hydrogen; palladium dihydroxide in water T=20°C; 15 h; atmospheric pressure;
参考文献
Uzawa, Hirotaka; Ito, Hiroki; Izumi, Masayuki; Tokuhisa, Hideo; Taguchi, Kazuhiro; Minoura, Norihiko
Tetrahedron, 2005 , vol. 61, # 24 p. 5895 - 5905
反应条件
1: NaOMe / methanol / 2 h / 20 °C 2: 95 percent / Pd/C / methanol / 0.5 h / 20 °C View Scheme
参考文献
Chemical Communications, , # 3 p. 229 - 230
反应条件
1: BF3*Et2O / CH2Cl2 / 72 h / 20 °C 2: NaOMe / methanol / 2 h / 20 °C 3: 95 percent / Pd/C / methanol / 0.5 h / 20 °C View Scheme
参考文献
Chemical Communications, , # 3 p. 229 - 230
反应条件
1: BF3*Et2O / CH2Cl2 / 72 h / 20 °C 2: NaOMe / methanol / 2 h / 20 °C 3: 95 percent / Pd/C / methanol / 0.5 h / 20 °C View Scheme
参考文献
Chemical Communications, , # 3 p. 229 - 230
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3 h / 20 °C 2: boron trifluoride diethyl etherate / dichloromethane / 2 h / -20 °C 3: palladium on activated charcoal; sodium tetrahydroborate / dichloromethane; methanol / 0.25 h / 0 °C 4: sodium methylate; methanol / 16 h / 20 °C View Scheme
参考文献
Chemistry of Materials, , vol. 25, # 20 p. 4122 - 4128
反应条件
methanol; sodium methylate T=20°C; 16 h;
参考文献
Chemistry of Materials, , vol. 25, # 20 p. 4122 - 4128
