3-(3-氨基苯)-1,3-恶唑烷-2-酮合成路线 (共 3 条)
反应条件
copper(l) iodide; potassium carbonate; 1,2-diamino-cyclohexane in 1,4-dioxane T=20 - 100°C; 18 h; Inert atmosphere;
参考文献
Bayer CropScience AG
Patent: US2011/245242 A1, 2011 ;
Location in patent: Page/Page column 38 ;
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran P=735.5 Torr; 1 h;
参考文献
Artico,M. et al.
Farmaco, Edizione Scientifica, 1971 , vol. 26, p. 771 - 783
反应条件
1: NaOEt / ethanol / 0.33 h / 75 °C 2: H2 / Pd-C / tetrahydrofuran / 1 h / 735.5 Torr View Scheme
参考文献
Artico,M. et al.
Farmaco, Edizione Scientifica, 1971 , vol. 26, p. 771 - 783