2-(2-噻吩基)苯并噻唑合成路线 (共 32 条)
反应条件
Iron (III) nitrate nonahydrate; dihydrogen peroxide T=50°C; 0.0833333 h;
参考文献
Das, Sudipto; Samanta, Suvendu; Maji, Swarup Kumar; Samanta, Partha Kumar; Dutta, Amit Kumar; Srivastava, Divesh N.; Adhikary, Bibhutosh; Biswas, Papu
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1090 - 1096
反应条件
air in chloroform T=20°C; 5 h;
参考文献
Carlson, Lauren J.; Welby, Jenna; Zebrowski, Kelly A.; Wilk, Matthew M.; Giroux, Rachel; Ciancio, Nicole; Tanski, Joseph M.; Bradley, Amy; Tyler, Laurie A.
Inorganica Chimica Acta, 2011 , vol. 365, # 1 p. 159 - 166
反应条件
in neat (no solvent) 1.5 h; Green chemistry; Time;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
反应条件
palladium diacetate T=60 - 75°C; 12 h; Ionic liquid;
参考文献
Kalkhambkar, Rajesh G.; Laali, Kenneth K.
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4212 - 4215
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
lithium chloride; PEPPSI-IPr catalyst in tetrahydrofuran; ethylene glycol dimethyl ether T=20°C; Kumada Coupling Reaction; 1 h; Product distribution / selectivity;
参考文献
Total Synthesis, Ltd.
Patent: US2007/73055 A1, 2007 ;
Location in patent: Page/Page column 13-14; 22 ;
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993
反应条件
PEPPSI™-IPr catalyst in tetrahydrofuran T=20°C; Kumada-Tamao-Corriu reaction; 24 h;
参考文献
Organ, Michael G.; Abdel-Hadi, Mirvat; Avola, Stephanie; Hadei, Niloufar; Nasielski, Joanna; O'Brien, Christopher J.; Valente, Cory
Chemistry - A European Journal, 2007 , vol. 13, # 1 p. 150 - 157
反应条件
Lawesson's reagent T=190°C; 0.0166667 h; microwave irradiation;
参考文献
Seijas, Julio A.; Vazquez-Tato, M. Pilar; Carballido-Reboredo, M. Raquel; Crecente-Campo, Jose; Romar-Lopez, Lucia
Synlett, 2007 , # 2 p. 313 - 317
反应条件
tri(n-propyl)amine; copper(l) iodide; 1,10-phenanthroline in 1,4-dioxane T=20 - 100°C; Wittig Olefination; 32.0833 h; Inert atmosphere;
参考文献
Yu, Hui; Zhang, Meishu; Li, Yuzhe
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8898 - 8903