2-(2-噻吩基)苯并噻唑合成路线 （共 32 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=140°C; 40 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
反应条件
di-isopropylperoxydicarbonate in benzene T=60°C; 5 h;
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
反应条件
1: in water; dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere; 2: With dipotassium peroxodisulfate 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
反应条件
di-isopropylperoxydicarbonate in benzene T=60°C; 5 h;
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
反应条件
in water T=70°C; 1 h; Microwave irradiationGreen chemistry;
参考文献
Panda, Siva S.; Ibrahim, Mohamed A.; Oliferenko, Alexander A.; Asiri, Abdullah M.; Katritzky, Alan R.
Green Chemistry, 2013 , vol. 15, # 10 p. 2709 - 2712
反应条件
triethylamine in ethanol 3 h; Heating;
参考文献
Elgemeie, Galal Eldin Hamza; Elghandour, Ahmed Hafez Hussein
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 281 - 284
反应条件
1: 65 percent / p-TsOH / benzene / Ambient temperature 2: 30 percent / diisopropyl peroxydicarbonate (DPDC) / benzene / 5 h / 60 °C View Scheme
参考文献
Emerson; Patrick
Journal of Organic Chemistry, 1949 , vol. 14, p. 790,795
反应条件
1: 80 percent / p-TsOH / benzene / Ambient temperature 2: 13 percent / benzene / 5 h / 60 °C View Scheme
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
反应条件
in methanol T=16 - 18°C; 72 h;
参考文献
Baichurina; Baichurin; Filippenko; Aboskalova; Berestovitskaya
Russian Journal of General Chemistry, 2012 , vol. 82, # 8 p. 1400 - 1408
Zh. Obshch. Khim., 2012 , vol. 82, # 8 p. 1321 - 1329,9
反应条件
1: SOCl2 / 1 h / 80 °C 2: toluene / 1 h / 20 °C View Scheme
参考文献
Rudrawar, Santosh; Kondaskar, Atul; Chakraborti, Asit K.
Synthesis, 2005 , # 15 art. no. Z05105SS, p. 2521 - 2526
