2-(2-噻吩基)苯并噻唑合成路线 (共 32 条)
反应条件
1: 65 percent / p-TsOH / benzene / Ambient temperature 2: 30 percent / diisopropyl peroxydicarbonate (DPDC) / benzene / 5 h / 60 °C View Scheme
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
反应条件
1: 40 percent / diisopropyl peroxydicarbonate (DPDC) / benzene / 5 h / 60 °C 2: 65 percent / p-TsOH / benzene / Ambient temperature 3: 30 percent / diisopropyl peroxydicarbonate (DPDC) / benzene / 5 h / 60 °C View Scheme
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
反应条件
in benzene T=60°C; 5 h;
参考文献
Leardini; Nanni; Santori; Zanardi
Tetrahedron, 1992 , vol. 48, # 19 p. 3961 - 3970
参考文献
Bogert; Stull
Journal of the American Chemical Society, 1926 , vol. 48, p. 251
反应条件
1: pyridine 2: ethanolic FeCl3 View Scheme
参考文献
Emerson; Patrick
Journal of Organic Chemistry, 1949 , vol. 14, p. 790,795
反应条件
in tetrahydrofuran Heating;
参考文献
George,B.; Papadopoulos,E.P.
Journal of Organic Chemistry, 1977 , vol. 42, p. 441 - 443
反应条件
pyridine hydrochloride
参考文献
Royer,R. et al.
Bulletin de la Societe Chimique de France, 1973 , p. 3017 - 3018
参考文献
Cohen,V.I.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 13 - 16
反应条件
oxygen 1.) 2-MeTHF, -125 deg C; 2.) -125 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lipshutz, Bruce H.; Kayser, Frank; Maullin, Nathalie
Tetrahedron Letters, 1994 , vol. 35, # 6 p. 815 - 818
反应条件
1: diethyl ether 2: Heating View Scheme
参考文献
Kornilov,M.Yu. et al.
Journal of Organic Chemistry USSR (English Translation), 1973 , vol. 9, p. 2596 - 2600
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, p. 2577 - 2582