1: With hydrogenchloride; sodium nitrite in water T=0°C; 0.0833333 h; Inert atmosphere; 2: With potassium iodide in water T=0 - 60°C; 3 h; Inert atmosphere;
NH4I; oxygen; acetic anhydride; NOBF4 in dichloromethane; acetic acid; trifluoroacetic acid T=25°C; 70 h; Title compound not separated from byproducts;
参考文献
Radner, Finn
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3548 - 3553