1-丁基-3-甲基咪唑甲磺酸盐合成路线 (共 16 条)
反应条件
in toluene 24 h; Reflux;
参考文献
Harjani, Jitendra R.; Farrell, Jeff; Garcia, M. Teresa; Singer, Robert D.; Scammells, Peter J.
Green Chemistry, 2009 , vol. 11, # 6 p. 821 - 829
反应条件
tri-n-hexyl amine in toluene T=40°C; 1 h;
参考文献
US2008/287684 A1, ;
Page/Page column 11 ;
反应条件
ammonia in water T=50°C; Cooling; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2010/217010 A1, 2010 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: methanesulfonic acid With Amberlyst A-26 (OH- form) in methanol; water T=20°C; 2: [bmim][I] in methanol
参考文献
Alcalde, Ermitas; Dinares, Immaculada; Ibanez, Anna; Mesquida, Neus
Molecules, 2012 , vol. 17, # 4 p. 4007 - 4027
反应条件
1-methyl-1H-imidazole
反应条件
in water T=25°C; 0.5 h;
参考文献
BASF Aktiengesellschaft
Patent: WO2006/27070 A1, 2006 ;
Location in patent: Page/Page column 31 ;
反应条件
in methanol 120 h; Reflux;
参考文献
Oh, Young-Ho; Jang, Hyeong Bin; Im, Suk; Song, Myoung Jong; Kim, So-Yeon; Park, Sung-Woo; Chi, Dae Yoon; Song, Choong Eui; Lee, Sungyul
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 418 - 422
反应条件
in trichloroethane, 1,1,1- 6 h; Heating;
参考文献
Brinchi; Germani; Savelli
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2027 - 2029
反应条件
1: 1-n-butyl-3-methylimidazolium chloride With potassium hydroxide in tetrahydrofuran Sonication; 2: NH4MeSO3 in water T=20°C;
参考文献
Tetrahedron Letters, , vol. 50, # 29 p. 4286 - 4288
反应条件
in methanol Ionic liquidsolid phase reaction;
参考文献
Dinares, Immaculada; Garcia De Miguel, Cristina; Ibanez, Anna; Mesquida, Neus; Alcalde, Ermitas
Green Chemistry, 2009 , vol. 11, # 10 p. 1507 - 1510