反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); tri-n-butyltin fluoride; triethylamine; [(t-Bu)3PH]BF4 / benzene / 24 h / 80 °C / Inert atmosphere 2: pyridine; sodium iodide / hexane; acetonitrile / 20 h / 20 °C 3: (R)-N-(5,5,4,4,3,3,2,2-octafluoropentyl)-tert-butanesulfinamide; 2,6-di-tert-butyl-phenol; 2,4-Dinitrobenzenesulfonic acid; sodium sulfate / toluene / -78 - -50 °C View Scheme
参考文献
Beck, Elizabeth M.; Hyde, Alan M.; Jacobsen, Eric N.
Organic Letters, 2011 , vol. 13, # 16 p. 4260 - 4263