4,6-二甲基-2-羟基嘧啶盐酸盐合成路线 （共 4 条）
反应条件
hydrogenchloride in ethanol T=90°C; 24 h;
参考文献
Gao, Lei; Liu, Qian; Ren, Sumei; Wan, Shengbiao; Jiang, Tao; Wong, Iris L. K.; Chow, Larry M. C.; Wang, Shixi
Journal of Carbohydrate Chemistry, 2012 , vol. 31, # 8 p. 620 - 633
反应条件
1: With sulfuric acid; nitric acid T=5 - 30°C; 2: With sodium hydroxide in water T=20°C; pH=2.5;
参考文献
Asubio Pharma Co., Ltd.
Patent: EP2151439 A1, 2010 ;
Location in patent: Page/Page column 18 ;
反应条件
trichlorophosphate 10 h; Heating;
参考文献
Bhasin; Arora, Ekta; Grover, Alka S.; Jyoti; Singh; Mehta; Bhasin, Aman K.K.; Jacob
Journal of Organometallic Chemistry, 2013 , vol. 732, p. 137 - 141
反应条件
1: 77 percent / phosphorus oxychloride / 10 h / Heating 2: 62 percent / conc. HI / 5 h / 20 °C View Scheme
参考文献
Vlad, Gabor; Horvath, Istvan T.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6550 - 6552
