2-氨基-6-喹啉羧酸乙酯合成路线 （共 4 条）
反应条件
ammonium acetate in ethyl acetate
参考文献
AJINOMOTO CO. INC
Patent: US2003/109547 A1, 2003 ;
US 20030109547 A1
反应条件
1.1: HCl / dioxane / 70 °C 2.1: m-chloroperbenzoic acid / CH2Cl2 / 20 °C 3.1: 1.87 g / POCl3 / CH2Cl2 / 50 °C 4.1: phenol / 0.17 h / 70 °C 4.2: 19 percent / ammonium acetate / 1 h View Scheme
参考文献
Sagi, Kazuyuki; Fujita, Koichi; Sugiki, Masayuki; Takahashi, Mitsuo; Takehana, Shunji; Tashiro, Kazumi; Kayahara, Takashi; Yamanashi, Masahiro; Fukuda, Yumiko; Oono, Seiji; Okajima, Akiko; Iwata, Seinosuke; Shoji, Masataka; Sakurai, Kuniya
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 5 p. 1487 - 1496
反应条件
1.1: m-chloroperbenzoic acid / CH2Cl2 / 20 °C 2.1: 1.87 g / POCl3 / CH2Cl2 / 50 °C 3.1: phenol / 0.17 h / 70 °C 3.2: 19 percent / ammonium acetate / 1 h View Scheme
参考文献
Sagi, Kazuyuki; Fujita, Koichi; Sugiki, Masayuki; Takahashi, Mitsuo; Takehana, Shunji; Tashiro, Kazumi; Kayahara, Takashi; Yamanashi, Masahiro; Fukuda, Yumiko; Oono, Seiji; Okajima, Akiko; Iwata, Seinosuke; Shoji, Masataka; Sakurai, Kuniya
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 5 p. 1487 - 1496
反应条件
1.1: 1.87 g / POCl3 / CH2Cl2 / 50 °C 2.1: phenol / 0.17 h / 70 °C 2.2: 19 percent / ammonium acetate / 1 h View Scheme
参考文献
Sagi, Kazuyuki; Fujita, Koichi; Sugiki, Masayuki; Takahashi, Mitsuo; Takehana, Shunji; Tashiro, Kazumi; Kayahara, Takashi; Yamanashi, Masahiro; Fukuda, Yumiko; Oono, Seiji; Okajima, Akiko; Iwata, Seinosuke; Shoji, Masataka; Sakurai, Kuniya
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 5 p. 1487 - 1496
