(R)-beta-甲基苯乙胺盐酸盐合成路线 (共 4 条)
反应条件
hydrogenchloride; ethanol; hydrogen; water-wet 5 palladium on carbon in water T=50 - 64°C; P=3878.71 - 4033.86 Torr; 3 h; Under nitrogen;
参考文献
Arnold, Macklin Brian; Bleisch, Thomas John; Cuff, George William; Ornstein, Paul Leslie; Zimmerman, Dennis Michael
Patent: US2003/225163 A1, 2003 ;
Location in patent: Page 8-12 ;
反应条件
hydrogen; Rh complex of bis(diphenylphosphino)-2,4-pentane in ethanol T=25°C; P=3750.3 Torr; 24 h; steel autoclave; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 98, # 6 p. 387 - 394
反应条件
sodium hydroxide; ethanol 1.6 h; Under nitrogen;
参考文献
Arnold, Macklin Brian; Bleisch, Thomas John; Cuff, George William; Ornstein, Paul Leslie; Zimmerman, Dennis Michael
Patent: US2003/225163 A1, 2003 ;
Location in patent: Page 8-12 ;
反应条件
sodium hydroxide; ethanol 1.6 h; Under nitrogen;
参考文献
Arnold, Macklin Brian; Bleisch, Thomas John; Cuff, George William; Ornstein, Paul Leslie; Zimmerman, Dennis Michael
Patent: US2003/225163 A1, 2003 ;
Location in patent: Page 8-12 ;