3-溴-2,6-二甲基吡啶合成路线 （共 10 条）
反应条件
sulfuric acid; bromine T=150°C; 18 h;
参考文献
Zimmermann, Nicole; Meggers, Eric; Schultz, Peter G.
Bioorganic Chemistry, 2004 , vol. 32, # 1 p. 13 - 25
反应条件
sulfuric acid; bromine T=155 - 175°C; 24 h;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 28, # 2 p. 59 - 60
参考文献
Gazzetta Chimica Italiana, , vol. 30 I, p. 94
反应条件
1: 29.8 g / KMnO4 / H2O / 12 h / 90 °C 2: thionyl chloride / 4 h / Heating 3: 25.0 g / 1 h / Heating View Scheme
参考文献
Zimmermann, Nicole; Meggers, Eric; Schultz, Peter G.
Bioorganic Chemistry, 2004 , vol. 32, # 1 p. 13 - 25
反应条件
potassium permanganate in water T=90°C; 12 h;
参考文献
Zimmermann, Nicole; Meggers, Eric; Schultz, Peter G.
Bioorganic Chemistry, 2004 , vol. 32, # 1 p. 13 - 25
反应条件
hydrogenchloride; zinc
参考文献
Bocchi
Gazzetta Chimica Italiana, 1900 , vol. 30 I, p. 94
参考文献
Bocchi
Gazzetta Chimica Italiana, 1900 , vol. 30 I, p. 94
反应条件
1: 3 h / 120 °C 2: 1) Ac2O, 2) 3percent HCl / 1) 120 deg C, 3 h, 2) 60 deg C, 4 h then 24 h, RT View Scheme
参考文献
Hanuza; Majczka; Waskowska; Oganowski; Andruszkiewicz; Ban-Oganowska; Lutz; Van Der Maas
Journal of Molecular Structure, 1997 , vol. 404, # 1-2 p. 33 - 45
反应条件
1: 3 h / 120 °C 2: 1) Ac2O, 2) 3percent HCl / 1) 120 deg C, 3 h, 2) 60 deg C, 4 h then 24 h, RT View Scheme
参考文献
Hanuza; Majczka; Waskowska; Oganowski; Andruszkiewicz; Ban-Oganowska; Lutz; Van Der Maas
Journal of Molecular Structure, 1997 , vol. 404, # 1-2 p. 33 - 45
反应条件
sulfuric acid; dihydrogen peroxide
1.) water, 0-10 deg C, 2.) water, 10-20 deg C, 20 min; Yield given. Multistep reaction;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 2 p. 626 - 633
