3-巯基-3-甲基-1-丁醇合成路线 （共 14 条）
反应条件
hydrogenchloride in methanol; diethyl ether
参考文献
Polak's Frutal Works B.V.; Douwe Egberts Koninklijke Tabaksfabriek-Koffiebranderijen-Theehandel N.V.
Patent: US3970689 A1, 1976 ;
反应条件
sodium in diethyl ether; ammonia T=-78°C; 1.5 h;
参考文献
Ohsugi, Shin-Ichi; Nishide, Kiyoharu; Node, Manabu
Tetrahedron, 2003 , vol. 59, # 11 p. 1859 - 1871
反应条件
1: piperidine / Heating 2: NaNH2 / liquid ammonia 3: (i) LiAlH4, Et2O, (ii) aq. NaOH View Scheme
参考文献
Sweetman; Vestling; Ticaric; Kelly; Field; Merryman; Jaffe
Journal of medicinal chemistry, 1971 , vol. 14, # 9 p. 868 - 872
反应条件
Saccharomyces cerevisiae MUCL43729 T=20°C; 150 h;
参考文献
Bailly, Sabine; Jerkovic, Vesna; Marchand-Brynaert, Jacqueline; Collin, Sonia
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 19 p. 7227 - 7234
反应条件
1: 65 percent / triethylamine / 18 h / 20 °C 2: aq. potassium carbonate / methanol / 0.25 h / 20 °C 3: Saccharomyces cerevisiae MUCL43729 / 150 h / 20 °C View Scheme
参考文献
Bailly, Sabine; Jerkovic, Vesna; Marchand-Brynaert, Jacqueline; Collin, Sonia
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 19 p. 7227 - 7234
反应条件
1: aq. potassium carbonate / methanol / 0.25 h / 20 °C 2: Saccharomyces cerevisiae MUCL43729 / 150 h / 20 °C View Scheme
参考文献
Bailly, Sabine; Jerkovic, Vesna; Marchand-Brynaert, Jacqueline; Collin, Sonia
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 19 p. 7227 - 7234
反应条件
1: 100 percent / EtONa / ethanol / 36 h / 20 - 50 °C 2: LiAlH4 / tetrahydrofuran / 1.5 h / Heating 3: 12.1 g / Na / liquid ammonia; diethyl ether / 1.5 h / -78 °C View Scheme
参考文献
Ohsugi, Shin-Ichi; Nishide, Kiyoharu; Node, Manabu
Tetrahedron, 2003 , vol. 59, # 11 p. 1859 - 1871
反应条件
1: LiAlH4 / tetrahydrofuran / 1.5 h / Heating 2: 12.1 g / Na / liquid ammonia; diethyl ether / 1.5 h / -78 °C View Scheme
参考文献
Ohsugi, Shin-Ichi; Nishide, Kiyoharu; Node, Manabu
Tetrahedron, 2003 , vol. 59, # 11 p. 1859 - 1871
反应条件
(i) LiAlH4, Et2O, (ii) aq. NaOH; Multistep reaction;
参考文献
Sweetman; Vestling; Ticaric; Kelly; Field; Merryman; Jaffe
Journal of medicinal chemistry, 1971 , vol. 14, # 9 p. 868 - 872
反应条件
pyridine; formic acid; acetic anhydride
参考文献
Polak's Frutal Works B.V.; Douwe Egberts Koninklijke Tabaksfabriek-Koffiebranderijen-Theehandel N.V.
Patent: US3970689 A1, 1976 ;
