BOC-L-2-氨基丁酸合成路线 (共 26 条)
反应条件
hydrogenchloride; sodium hydroxide in water; tert-butyl alcohol
反应条件
sodium hydroxide in methanol; water Heatingother reagent, solvent; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
2-(tert-butoxycarbonyloxyimino)-2-phenylacetonitrile; triethylamine in water; acetone 4 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3186 - 3194
反应条件
hydrogen; 10 palladium on active carbon in methanol P=2068.6 Torr; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4817 - 4820
反应条件
Bacillus licheniformis in water T=30°C; pH=7.5; 4 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 13 p. 1995 - 1999
反应条件
lithium hydroxide in tetrahydrofuran; methanol; water
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2121 - 2124
反应条件
alkali in 1,4-dioxane; water
参考文献
Phytochemistry, , vol. 62, # 7 p. 1133 - 1140
反应条件
1: 95 percent / NaOH / 2-methyl-propan-2-ol; H2O 2: 95 percent / 1,3-dicyclohexylcarbodiimid, N,N-dimethylaminopyridine / CH2Cl2 3: Raney Ni / ethanol 4: 99 percent / LiOH / H2O; tetrahydrofuran; methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2121 - 2124
反应条件
1: Et3N / CH2Cl2 / 0.5 h / 0 °C 2: 13.0 g / Et3N / CH2Cl2 / 1 h / 0 °C 3: LDA, LiCl / tetrahydrofuran / 1 h / 0 °C 4: NaOH / H2O; methanol / Heating; other reagent, solvent View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
1: 13.0 g / Et3N / CH2Cl2 / 1 h / 0 °C 2: LDA, LiCl / tetrahydrofuran / 1 h / 0 °C 3: NaOH / H2O; methanol / Heating; other reagent, solvent View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673