BOC-L-2-氨基丁酸合成路线 （共 26 条）
反应条件
1: LDA, LiCl / tetrahydrofuran / 1 h / 0 °C 2: NaOH / H2O; methanol / Heating; other reagent, solvent View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile 24 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 64, # 13 p. 4610 - 4616
反应条件
1: 73 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / tetrahydrofuran / 0 °C 2: 74 percent / PPh3, diethylazodicarboxylate / tetrahydrofuran / 0 °C 3: 33 percent / CuBr*Me2S / tetrahydrofuran; toluene / 16 h / -20 °C 4: 1.) CF3CO2H; 2.) 6N HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3761 - 3764
反应条件
1: 74 percent / PPh3, diethylazodicarboxylate / tetrahydrofuran / 0 °C 2: 33 percent / CuBr*Me2S / tetrahydrofuran; toluene / 16 h / -20 °C 3: 1.) CF3CO2H; 2.) 6N HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3761 - 3764
反应条件
1: 33 percent / CuBr*Me2S / tetrahydrofuran; toluene / 16 h / -20 °C 2: 1.) CF3CO2H; 2.) 6N HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3761 - 3764
反应条件
1: 95 percent / 1,3-dicyclohexylcarbodiimid, N,N-dimethylaminopyridine / CH2Cl2 2: Raney Ni / ethanol 3: 99 percent / LiOH / H2O; tetrahydrofuran; methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2121 - 2124
反应条件
1: Raney Ni / ethanol 2: 99 percent / LiOH / H2O; tetrahydrofuran; methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 14 p. 2121 - 2124
反应条件
triethylamine in 1,4-dioxane; water 4 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 47, # 29 p. 5453 - 5462
反应条件
hydrogenchloride; trifluoroacetic acid Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3761 - 3764
反应条件
trifluoroacetic acid
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3761 - 3764
