5,11-二氢二苯并[b,e][1,4]噁氮杂卓合成路线 （共 4 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; L-proline in water; dimethyl sulfoxide T=90°C; 48 h;
参考文献
Guo, Lei; Li, Ben; Huang, Wenlong; Pei, Gang; Ma, Dawei
Synlett, 2008 , # 12 p. 1833 - 1836
反应条件
1: 80 percent / HCl; Fe / propan-2-ol / 17 h / 60 °C 2: 86 percent / NaO-t-Bu; K2CO3; P(t-Bu)3 / Pd2(dba)3 / toluene / 2.5 h / 95 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 644 - 647
反应条件
1: 96 percent / K2CO3 / acetonitrile / 2 h / 70 °C 2: 80 percent / HCl; Fe / propan-2-ol / 17 h / 60 °C 3: 86 percent / NaO-t-Bu; K2CO3; P(t-Bu)3 / Pd2(dba)3 / toluene / 2.5 h / 95 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 644 - 647
反应条件
1: 96 percent / K2CO3 / acetonitrile / 2 h / 70 °C 2: 80 percent / HCl; Fe / propan-2-ol / 17 h / 60 °C 3: 86 percent / NaO-t-Bu; K2CO3; P(t-Bu)3 / Pd2(dba)3 / toluene / 2.5 h / 95 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 644 - 647
