反应条件
1: sodium / 1.) EtOH, 45 deg C, 20 min, 2.) EtOH, a) from 25 deg C to 70 deg C, b) 85 deg C, 1 h 2: 85percent aq. KOH / 2 h / 90 - 100 °C 3: 130 - 195 °C 4: 65 percent / BH3 / tetrahydrofuran / 1 h / 25 °C 5: 66 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / 25 °C 6: 83 percent / diethyl ether / 0 °C 7: 81 percent / pyridinium chlorochromate / CH2Cl2 / 3 h View Scheme
参考文献
Walker, Michael A.; Johnson, Timothy; Ma, Zhuping; Banville, Jacques; Remillard, Roger; Kim, Oak; Zhang, Yunhui; Staab, Andrew; Wong, Henry; Torri, Albert; Samanta, Himadri; Lin, Zeyu; Deminie, Carol; Terry, Brian; Krystal, Mark; Meanwell, Nicholas
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 11 p. 2920 - 2924
