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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
条叶蓟素
合成路线
（共 10 条）
51145-78-9
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 2: pyridine / Heating 3: AlCl3 / acetonitrile / 1.5 h / 60 °C 4: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
22248-14-2
2,3,4-三甲氧基-6-羟基苯乙酮
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: pyridine / 3 h / 120 °C 2: KOH, pyridine / 4 h / 60 °C 3: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C 4: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 5: pyridine / Heating 6: AlCl3 / acetonitrile / 1.5 h / 60 °C 7: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
55274-37-8
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C 2: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 3: pyridine / Heating 4: AlCl3 / acetonitrile / 1.5 h / 60 °C 5: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
6962-57-8
1-(3,6-二羟基-2,4-二甲氧基苯基)-乙酮
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: K2CO3 / acetone / Heating 2: pyridine / 3 h / 120 °C 3: KOH, pyridine / 4 h / 60 °C 4: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C 5: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 6: pyridine / Heating 7: AlCl3 / acetonitrile / 1.5 h / 60 °C 8: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
1486-54-0
3,4-二(苄氧基)苯甲酰氯
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: pyridine / 3 h / 120 °C 2: KOH, pyridine / 4 h / 60 °C 3: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C 4: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 5: pyridine / Heating 6: AlCl3 / acetonitrile / 1.5 h / 60 °C 7: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
55274-36-7
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: KOH, pyridine / 4 h / 60 °C 2: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C 3: 97 percent / H2 / 10percent Pd/C / methanol; ethyl acetate 4: pyridine / Heating 5: AlCl3 / acetonitrile / 1.5 h / 60 °C 6: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
97389-87-2
→
反应条件
34334-69-5
条叶蓟素
反应条件
hydrogenchloride in methanol 4 h; Heating; Yield given;
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
51145-79-0
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: pyridine / Heating 2: AlCl3 / acetonitrile / 1.5 h / 60 °C 3: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
97389-88-3
→
反应条件
34334-69-5
条叶蓟素
反应条件
1: AlCl3 / acetonitrile / 1.5 h / 60 °C 2: 6 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Horie, Tokunaru; Tsukayama, Masao; Kourai, Hiroki; Yokoyama, Chieko; Furukawa, Masayuki; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2256 - 2262
34334-69-5
条叶蓟素
+
14031-35-7
→
反应条件
41365-32-6
甲基条叶蓟素
反应条件
Ocimum basilicum L. phenylpropanoid–flavonoid O-methyltransferase 1; magnesium chloride in aq. buffer pH=8.5; Enzymatic reaction; Kinetics;
参考文献
Berim, Anna; Gang, David R.
Phytochemistry, 2013 , vol. 92, p. 33 - 41
