(2S,5S)-2,5-己二醇合成路线 （共 27 条）
反应条件
1: Jones reagent 2: BH3*SMe2 / (R)-B-methyl-4,5,5-triphenyl-1,3,2-oxazaborolidine / tetrahydrofuran / 0 °C 3: H2 / Pt/C / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 6 p. 1091 - 1094
反应条件
1: BH3*SMe2 / (R)-B-methyl-4,5,5-triphenyl-1,3,2-oxazaborolidine / tetrahydrofuran / 0 °C 2: H2 / Pt/C / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 6 p. 1091 - 1094
参考文献
Solladie, Guy; Huser, Nathalie; Garcia-Ruano, Jose Luis; Adrio, Javier; Carmen Carreno; Tito, Amelia
Tetrahedron Letters, 1994 , vol. 35, # 29 p. 5297 - 5300
参考文献
Tetrahedron: Asymmetry, , vol. 5, # 4 p. 657 - 664
反应条件
hydrogen; platinum on activated charcoal in methanol Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 38, # 6 p. 1091 - 1094
参考文献
Journal of Organic Chemistry, , vol. 58, # 23 p. 6483 - 6485
反应条件
mannose; Bacillus subtilis glucose dehydrogenase; NADPH T=30°C; pH=7.5; 3 h; Enzymatic reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 7 p. 1540 - 1550
反应条件
Candida antarctica lipase B in toluene T=20°C; 0.0416667 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 12, # 23 p. 6053 - 6061
反应条件
HCl buffer; isopropyl alcohol; tri-(hydroxymethyl)-methylamine T=30°C; pH=8; 24 h; Title compound not separated from byproducts.;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 16 p. 1954 - 1958
反应条件
barium dihydroxide; methanesulfonic acid 1) MeOH, 16 h, reflux, 2) MeOH, 4 h, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 33, # 37 p. 5327 - 5330
