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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
34352-92-6
合成路线
（共 26 条）
904744-28-1
→
反应条件
34352-92-6
反应条件
MS 4 Angstroem; zinc trifluoromethanesulfonate in toluene T=90°C; 3 h;
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
14559-87-6
异丙烯基硼酸
+
5111-65-9
2-溴-6-甲氧基萘
→
反应条件
34352-92-6
反应条件
cis,cis,cis-tetrakis[(diphenylphosphanyl)methyl]cyclopentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in xylene T=130°C; Suzuki reaction; 20 h;
参考文献
Peyroux, Eugenie; Berthiol, Florian; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2004 , # 5 p. 1075 - 1082
34352-83-5
→
反应条件
34352-92-6
反应条件
pyridine; trichlorophosphate in dichloromethane T=0 - 25°C;
参考文献
Nandanan; Jayachandran; Phukan, Prodeep; Pais, Godwin C. G.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 12 p. 1221 - 1227
5111-65-9
2-溴-6-甲氧基萘
+
145624-59-5
→
反应条件
34352-92-6
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
参考文献
Rivera, Isaac; Colberg, Juan C.; Soderquist, John A.
Tetrahedron Letters, 1992 , vol. 33, # 46 p. 6919 - 6922
904744-76-9
→
反应条件
34352-92-6
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / -78 °C 1.2: 78 percent / tetrahydrofuran; hexane / -78 °C 2.1: n-BuLI / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 88 percent / tetrahydrofuran; hexane / -78 °C 3.1: 90 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 1 h / 20 °C 4.1: 81 percent / MS 4 Angstroem / Zn(OTf)2 / toluene / 3 h / 90 °C View Scheme
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
904744-77-0
→
反应条件
34352-92-6
反应条件
1: 90 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 1 h / 20 °C 2: 81 percent / MS 4 Angstroem / Zn(OTf)2 / toluene / 3 h / 90 °C View Scheme
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
7507-86-0
2-溴-5-甲氧基苯甲醛
→
反应条件
34352-92-6
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 1.2: 76 percent / tetrahydrofuran; hexane / 0 °C 2.1: n-BuLi / tetrahydrofuran; hexane / -78 °C 2.2: 78 percent / tetrahydrofuran; hexane / -78 °C 3.1: n-BuLI / tetrahydrofuran; hexane / 0.5 h / -78 °C 3.2: 88 percent / tetrahydrofuran; hexane / -78 °C 4.1: 90 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 1 h / 20 °C 5.1: 81 percent / MS 4 Angstroem / Zn(OTf)2 / toluene / 3 h / 90 °C View Scheme
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
591-31-1
3-甲氧基苯甲醛
→
反应条件
34352-92-6
反应条件
1.1: 73 percent / Br2 / acetic acid / 24 h / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 2.2: 76 percent / tetrahydrofuran; hexane / 0 °C 3.1: n-BuLi / tetrahydrofuran; hexane / -78 °C 3.2: 78 percent / tetrahydrofuran; hexane / -78 °C 4.1: n-BuLI / tetrahydrofuran; hexane / 0.5 h / -78 °C 4.2: 88 percent / tetrahydrofuran; hexane / -78 °C 5.1: 90 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 1 h / 20 °C 6.1: 81 percent / MS 4 Angstroem / Zn(OTf)2 / toluene / 3 h / 90 °C View Scheme
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
610312-60-2
→
反应条件
34352-92-6
反应条件
1.1: n-BuLI / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: 88 percent / tetrahydrofuran; hexane / -78 °C 2.1: 90 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 1 h / 20 °C 3.1: 81 percent / MS 4 Angstroem / Zn(OTf)2 / toluene / 3 h / 90 °C View Scheme
参考文献
Lin, Ming-Yuan; Das, Arindam; Liu, Rai-Shung
Journal of the American Chemical Society, 2006 , vol. 128, # 29 p. 9340 - 9341
128333-21-1
→
反应条件
34352-92-6
反应条件
manganese(IV) oxide in various solvent(s) T=180°C; 120 h;
参考文献
Shishido, Kozo; Yamashita, Akitake; Hiroya, Kou; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 469 - 475
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