反应条件
1: 1.) NaH / 1) DMF, 0 deg C, 1 h; 2) DMF, 2 h, 0 deg C 2: 97.9 percent / CF3COOH / H2O / 0.25 h / 20 °C 3: H2 / palldium on carbon / methanol; H2O / 16 h / 20 °C / 2585.7 Torr 4: H2O / 4 h / 20 °C View Scheme
参考文献
Spiers, Ian D.; Schwalbe, Carl H.; Blake, Alexander J.; Solomons, Kevin R.H.; Freeman, Sally
Carbohydrate Research, 1997 , vol. 302, # 1-2 p. 43 - 51
