Rinkes
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 643,648
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 991
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Dann
Chemische Berichte, 1943 , vol. 76, p. 419,428
Rinkes
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 643,648
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 991
Full Text Show Details
Dann
Chemische Berichte, 1943 , vol. 76, p. 419,428
1: 4-oxo-4H-1-benzopyran With (2,2,6,6-tetramethylpiperidine)2Zn·2MgCl2·2LiCl in tetrahydrofuran
T=-30°C; 1 h; Inert atmosphere;
2: 2-Iodothiophene With bis(dibenzylideneacetone)-palladium(0); P(2-furyl)3 in tetrahydrofuran
T=25°C; Negishi cross-coupling reaction; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Klier, Lydia; Bresser, Tomke; Nigst, Tobias A.; Karaghiosoff, Konstantin; Knochel, Paul
Journal of the American Chemical Society, 2012 , vol. 134, # 33 p. 13584 - 13587
sodium in tetrahydrofuran
T=35 - 90°C; 16 h; Inert atmosphere;
参考文献
RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY; PROVID PHARMACEUTICALS INC.; EBRIGHT, Richard H.; EBRIGHT, Yon W.; SHEN, Juan; BACCI, James; HIEBEL, Anne-Cecile; SOLVIBILE, William; SELF, Christopher; OLSON, Gary
Patent: WO2013/192352 A1, 2013 ;
Location in patent: Page/Page column 93 ;