2-氨基-5-丙基噻吩-3-羧酸甲酯合成路线 (共 2 条)
反应条件
sulfur; triethylamine in N,N-dimethyl-formamide T=50°C;
参考文献
LG LIFE SCIENCES LTD.
Patent: US2011/166121 A1, 2011 ;
Location in patent: Page/Page column 114 ;
US 20110166121 A1
反应条件
1: α-cyanoacetic acid methyl ester With octasulfur; triethylamine in N,N-dimethyl-formamide 0.166667 h; 2: pentanal in N,N-dimethyl-formamide T=20 - 50°C; 20 h;
参考文献
WO2006/79916 A1, ;
Page/Page column 94-95 ;