4-甲基-1-丁基吡啶四氟硼酸盐合成路线 （共 5 条）
反应条件
1: in acetonitrile T=60°C; 48 h; Inert atmosphere; 2: With sodium tetrafluoroborate in water; acetonitrile T=60°C;
参考文献
Dos Santos Castro, Kelly L.; De Lima, Paulo G.; E Miranda, Leandro S.M.; De Souza, Rodrigo O.M.A.
Tetrahedron Letters, 2011 , vol. 52, # 32 p. 4168 - 4171
反应条件
sodium tetrafluoroborate T=70°C; 336 h;
参考文献
Solvent Innovation GmbH
Patent: EP1182197 A1, 2002 ;
Location in patent: Page 13, 14 ;
反应条件
Amberlyst A-26 (BF4- form) in methanol
参考文献
Alcalde, Ermitas; Dinares, Immaculada; Ibanez, Anna; Mesquida, Neus
Molecules, 2012 , vol. 17, # 4 p. 4007 - 4027
反应条件
tetrafluoroboric acid in water T=20°C; 0.333333 h;
参考文献
MERCK PATENT GMBH
Patent: WO2006/7912 A1, 2006 ;
Location in patent: Page/Page column 20-21 ;
反应条件
alkali metal tetrafluoroborate T=150°C; 0.75 h; Microwave irradiationCoolingneat (no solvent);
参考文献
Combinatorial Chemistry and High Throughput Screening, , vol. 15, # 5 p. 427 - 432
