2-(三氟甲基)乙酰苯胺合成路线 （共 23 条）
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2352
反应条件
tert.-butylhydroperoxide; copper(II) bis(trifluoromethanesulfonate) in water; acetonitrile T=20°C; 2.5 h; other aromatic compounds; Mechanism;
参考文献
Tetrahedron Letters, , vol. 32, # 51 p. 7525 - 7528
反应条件
in acetonitrile 4.5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 2 p. 447 - 452
反应条件
1: H2SO4; HNO3 2: aq.-ethanolic NaOH 3: acetic acid; sulfuric acid; aqueous sodium nitrite solution; aqueous potassium iodide solution 4: copper-powder / 300 °C 5: tin; aq.-ethanolic HCl View Scheme
参考文献
Pettit; Tatlow
Journal of the Chemical Society, 1951 , p. 3459,3463
Journal of the Chemical Society, 1954 , p. 1071,1074
反应条件
sulfuric acid; nitric acid
参考文献
Pettit; Tatlow
Journal of the Chemical Society, 1951 , p. 3459,3463
Journal of the Chemical Society, 1954 , p. 1071,1074
反应条件
1.1: thionyl chloride / methanol / 1.5 h / 75 °C 2.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C 2.2: 3 h / 0 - 60 °C View Scheme
参考文献
Zhang, Li-Sheng; Chen, Kang; Chen, Guihua; Li, Bi-Jie; Luo, Shuang; Guo, Qing-Yun; Wei, Jiang-Bo; Shi, Zhang-Jie
Organic Letters, 2013 , vol. 15, # 1 p. 10 - 13
反应条件
1: H2SO4; HNO3 2: aq.-ethanolic NaOH 3: acetic acid; sulfuric acid; aqueous sodium nitrite solution; aqueous potassium iodide solution 4: H2SO4 View Scheme
参考文献
Pettit; Tatlow
Journal of the Chemical Society, 1951 , p. 3459,3463
Journal of the Chemical Society, 1954 , p. 1071,1074
反应条件
1.1: thionyl chloride / methanol / 1.5 h / 75 °C 2.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C 2.2: 3 h / 0 - 60 °C View Scheme
参考文献
Zhang, Li-Sheng; Chen, Kang; Chen, Guihua; Li, Bi-Jie; Luo, Shuang; Guo, Qing-Yun; Wei, Jiang-Bo; Shi, Zhang-Jie
Organic Letters, 2013 , vol. 15, # 1 p. 10 - 13
反应条件
1: H2SO4; HNO3 2: aq.-ethanolic NaOH View Scheme
参考文献
Journal of the Chemical Society, , p. 3459,3463
Journal of the Chemical Society, , p. 1071,1074
反应条件
1: 79 percent / K2CO3, Cu2Br2 / 26 h / 170 - 180 °C
2: 9.6 percent / KOH / 6 h / Heating
View Scheme
参考文献
Murakami; Watanabe; Hagiwara; Akiyama; Ishii
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 8 p. 1281 - 1286
