N^e-苄氧羰基-D-赖氨酸合成路线 (共 6 条)
反应条件
L-amino acid oxide ase-substance from crotalus adamanteus
参考文献
Journal of the American Chemical Society, , vol. 80, p. 953,954, 957
反应条件
toluene-4-sulfonic acid in 1,4-dioxane
参考文献
Bulletin of the Chemical Society of Japan, , vol. 51, p. 1899 - 1900
反应条件
copper carbonate hydroxide; sodium hydroxide 1.) H2O, reflux, 2.5 h, 2.) RT, overnight; Yield given. Multistep reaction;
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 914 - 934
反应条件
1: 98 percent / NaOH / dioxane; H2O / 1.5 h / 4 °C 2: 1.) H2, 2.) aq. NaHCO3 / 1.) Pd on carbon / 1) ethanol, overnight; 2) dioxane, ice-bath, 70 min View Scheme
参考文献
Marsh, Ian R.; Bradley, Mark; Teague, Simon J.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6199 - 6203
反应条件
1: 91 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature 2: H2 / 5percent Pd/C / methanol; H2O / 24 h / 2585.7 Torr View Scheme
参考文献
Acosta, C. Kirk; Bahr, Martin L.; Burdett, James E.; Cessac, James W.; Martinez, Rudy A.; et al.
Journal of Chemical Research, Miniprint, 1991 , # 5 p. 914 - 934
反应条件
1: 91 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature 2: H2 / 5percent Pd/C / methanol; H2O / 24 h / 2585.7 Torr 3: dimethylformamide / 120 h / Ambient temperature View Scheme
参考文献
Acosta, C. Kirk; Bahr, Martin L.; Burdett, James E.; Cessac, James W.; Martinez, Rudy A.; et al.
Journal of Chemical Research, Miniprint, 1991 , # 5 p. 914 - 934