2-氨基-2-甲基-1-苯基-丙-1-醇合成路线 （共 11 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 5 h; Heating;
参考文献
Colvin, Ernest W.; Beck, Albert K.; Seebach, Dieter
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2264 - 2271
反应条件
phosphate buffer; potassium chloride in ethanol T=30°C; cotrolled potential electrolysis, cathod: Hg, vs. S.C.E.;
参考文献
Ohmori, Hidenobu; Furusako, Shoji; Kashu, Mieko; Ueda, Chihiro; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3345 - 3353
反应条件
citrate buffer; potassium chloride in ethanol T=30°C; cotrolled potential electrolysis, cathod: Hg, vs. S.C.E.;
参考文献
Ohmori, Hidenobu; Furusako, Shoji; Kashu, Mieko; Ueda, Chihiro; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3345 - 3353
反应条件
potassium carbonate in methanol; water 2 h; Heating;
参考文献
Nordlander, Eric J.; Payne, Mark J.; Njoroge, George F.; Balk, Michael A.; Laikos George D.; Vishwanath, Vasanth M.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4107 - 4111
反应条件
1: 97 percent / H2 / Pd-C / ethanol / 12 h / 2275.5 Torr 2: 60 percent / K2CO3 / methanol; H2O / 2 h / Heating View Scheme
参考文献
Nordlander, Eric J.; Payne, Mark J.; Njoroge, George F.; Balk, Michael A.; Laikos George D.; Vishwanath, Vasanth M.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4107 - 4111
反应条件
1: 25 percent / tetra(n-butyl)ammonium fluoride / tetrahydrofuran / -78 - 25 °C 2: 66 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Colvin, Ernest W.; Beck, Albert K.; Seebach, Dieter
Helvetica Chimica Acta, 1981 , vol. 64, # 7 p. 2264 - 2271
反应条件
acetic acid 12 h; Ambient temperature; Yield given;
参考文献
Amouroux, Roger; Axiotis, Georges P.
Synthesis, 1981 , # 4 p. 270 - 272
反应条件
phosphorus; hydrogen iodide
参考文献
Zenitz; Macks; Moore
Journal of the American Chemical Society, 1948 , vol. 70, p. 955
反应条件
1: aqueous hydriodic acid; phosphorus 3: anschliessend mit wss. Aethanol View Scheme
参考文献
Zenitz; Macks; Moore
Journal of the American Chemical Society, 1948 , vol. 70, p. 955
反应条件
1: aqueous hydriodic acid; phosphorus
3: anschliessend mit wss. Aethanol
4: platinum; acetic acid / Hydrogenation
View Scheme
参考文献
Zenitz; Macks; Moore
Journal of the American Chemical Society, 1948 , vol. 70, p. 955
