双(二叔丁基苯基膦)二氯化钯(II)合成路线 (共 2 条)
反应条件
in dichloromethane Pt complex and org. compd. stirred together in CH2Cl2 for 3 h; removal of solvent, rerystn. (CH2Cl2-MeOH); elem. anal.;
参考文献
Inorganic Chemistry, , vol. 20, p. 3611 - 3616
反应条件
in methanol (N2); dropwise addn. of a soln. of phosphine to a soln. of Pd-complex; stirring for 1 h; filtration; washing with methanol; 3 times recrystn. from MeOH/CH2Cl2 (1:1); elem. anal.;
参考文献
Journal of Physical Chemistry, , vol. 94, # 16 p. 6255 - 6263