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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙基硼酸
合成路线
（共 30 条）
34420-17-2
苯乙基硼酸
+
106-49-0
对甲苯胺
→
反应条件
1739-02-2
反应条件
1: p-toluidine With pyridine; copper diacetate in 1,4-dioxane Chan-Lam-Evans reaction; 0.25 h; Reflux; 2: Phenethylboronic acid in 1,4-dioxane Chan-Lam-Evans reaction;
参考文献
Larrosa, Marta; Guerrero, Cesar; Rodriguez, Ramon; Cruces, Jacobo
Synlett, 2010 , # 14 art. no. D07810ST, p. 2101 - 2105
34420-17-2
苯乙基硼酸
→
反应条件
10270-27-6
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
34420-17-2
苯乙基硼酸
→
反应条件
1714-09-6
反应条件
1: With tetrakis(triphenylphosphine) palladium(0); caesium carbonate in tetrahydrofuran T=100°C; 1 h; Inert atmosphere; 2: With boron trifluoride diethyl etherate in dichloromethane T=20°C; 1 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yanzhong; Wang, Chengyu; Kong, Lingkai; Li, Yanli
European Journal of Organic Chemistry, 2014 , vol. 2014, # 17 p. 3556 - 3560
34420-17-2
苯乙基硼酸
+
104-94-9
对甲氧基苯胺
→
反应条件
2405-59-6
反应条件
1: 4-methoxy-aniline With pyridine; copper diacetate in 1,4-dioxane Chan-Lam-Evans reaction; 0.25 h; Reflux; 2: Phenethylboronic acid in 1,4-dioxane Chan-Lam-Evans reaction;
参考文献
Larrosa, Marta; Guerrero, Cesar; Rodriguez, Ramon; Cruces, Jacobo
Synlett, 2010 , # 14 art. no. D07810ST, p. 2101 - 2105
104-92-7
4-溴苯甲醚
+
34420-17-2
苯乙基硼酸
→
反应条件
14310-21-5
1-甲氧基-4-(2-苯基乙基)-苯
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
34420-17-2
苯乙基硼酸
+
66107-29-7
4-甲氧基三氟甲烷磺酸苯酯
→
反应条件
14310-21-5
1-甲氧基-4-(2-苯基乙基)-苯
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
34420-17-2
苯乙基硼酸
→
反应条件
7726-45-6
5-苯基戊腈
反应条件
1: toluene / 4 h / |Dean-Stark; |Inert atmosphere 2: potassium hydroxide / toluene / 4 h / |Dean-Stark; |Inert atmosphere; |Reflux 3: [Ir(dF(CF3)ppy)2(bpy)](PF6) / acetone; methanol / 24 h / 20 °C / |Inert atmosphere; |UV-irradiation View Scheme
参考文献
Yasu, Yusuke; Koike, Takashi; Akita, Munetaka
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 18 p. 3414 - 3420
2905-62-6
3,5-二氯苯甲酰氯
+
34420-17-2
苯乙基硼酸
→
反应条件
898788-84-6
1-(3,5-二氯苯基)-3-苯基-1-丙酮
反应条件
potassium phosphate; bis-triphenylphosphine-palladium(II) chloride in toluene T=70°C;
参考文献
Mallari, Jeremy P.; Shelat, Anang; Kosinski, Aaron; Caffrey, Conor R.; Connelly, Michele; Zhu, Fangyi; McKerrow, James H.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 9 p. 2883 - 2885
90-90-4
4-溴苯甲酰苯
+
34420-17-2
苯乙基硼酸
→
反应条件
91036-10-1
4-2-苯乙基苯甲酮
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
34420-17-2
苯乙基硼酸
→
反应条件
40164-53-2
反应条件
[Ru(2,2′-bipyridine)3][hexafluorophosphate]2; hydroxybenziodoxole; sodium carbonate in dichloromethane; water 12 h;
参考文献
Huang, Hanchu; Zhang, Guojin; Gong, Li; Zhang, Shuaiyan; Chen, Yiyun
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2280 - 2283
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