1,2,3,5,6,7-六氢-二环戊烷并[b,e]吡啶合成路线 (共 10 条)
反应条件
hydroxylamine hydrochloride in ethanol; water
参考文献
John Wyeth and Brother Limited
Patent: US3963722 A1, 1976 ;
反应条件
hydroxylamine hydrochloride in ethanol; water
参考文献
John Wyeth and Brother Limited
Patent: US4031102 A1, 1977 ;
反应条件
hydroxylamine hydrochloride in ethanol; water
参考文献
John Wyeth and Brother Ltd.
Patent: US4085215 A1, 1978 ;
反应条件
tetrahydropyridine hydrochloride in toluene T=200°C; 2 h; autoclave;
参考文献
Vijn; Arts; Green; Castelijns
Synthesis, 1994 , # 6 p. 573 - 578
反应条件
ammonia; hydrogen; nickel; ruthenium
参考文献
Kriven'ko, A. P.; Fedotova, O. V.; Nikolaeva, T. G.; Komyagin, N. T.; Yudovich, L. M.; et. al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 8 p. 901 - 905
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 8 p. 1094 - 1099
反应条件
in 1,2,3,4-tetrahydro-naphthalene 24 h; Heating;
参考文献
Tabyaoui, B.; Aubert, T.; Farnier, M.; Guilard, R.
Synthetic Communications, 1988 , vol. 18, # 13 p. 1475 - 1482
反应条件
1: 80 percent / sodium azide / dimethylsulfoxide / 1.) 10 deg C, 1 h, 2.) room temperature, 4 h 2: 85 percent / toluene / 2 h / Ambient temperature 3: 80 percent / 1,2,3,4-tetrahydro-naphthalene / 24 h / Heating View Scheme
参考文献
Tabyaoui, B.; Aubert, T.; Farnier, M.; Guilard, R.
Synthetic Communications, 1988 , vol. 18, # 13 p. 1475 - 1482
反应条件
1: POCl3 / CH2Cl2 / 2 h / Ambient temperature 2: 80 percent / sodium azide / dimethylsulfoxide / 1.) 10 deg C, 1 h, 2.) room temperature, 4 h 3: 85 percent / toluene / 2 h / Ambient temperature 4: 80 percent / 1,2,3,4-tetrahydro-naphthalene / 24 h / Heating View Scheme
参考文献
Tabyaoui, B.; Aubert, T.; Farnier, M.; Guilard, R.
Synthetic Communications, 1988 , vol. 18, # 13 p. 1475 - 1482
反应条件
1: 85 percent / toluene / 2 h / Ambient temperature 2: 80 percent / 1,2,3,4-tetrahydro-naphthalene / 24 h / Heating View Scheme
参考文献
Tabyaoui, B.; Aubert, T.; Farnier, M.; Guilard, R.
Synthetic Communications, 1988 , vol. 18, # 13 p. 1475 - 1482
反应条件
ammonium acetate; acetic acid
参考文献
Colonge et al.
Bulletin de la Societe Chimique de France, 1957 , p. 447