3-(二甲基氨基)-4-甲氧基苯甲酸甲酯合成路线 （共 2 条）
反应条件
sodium tetrahydroborate; sulfuric acid in tetrahydrofuran; water T=0 - 20°C;
参考文献
Ohtsu, Hironori; Itokawa, Hideji; Xiao, Zhiyan; Su, Ching-Yuan; Shih, Charles C.-Y.; Chiang, Tzuying; Chang, Eugene; Lee, YiFen; Chiu, Shang-Yi; Chang, Chawnshang; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5083 - 5090
反应条件
1: 82 percent / DIBAL-H / CH2Cl2; toluene / 0.5 h / 0 °C
2: 74 percent / (COCl)2; DMSO; Et3N / CH2Cl2 / -78 - 0 °C
View Scheme
参考文献
Ohtsu, Hironori; Itokawa, Hideji; Xiao, Zhiyan; Su, Ching-Yuan; Shih, Charles C.-Y.; Chiang, Tzuying; Chang, Eugene; Lee, YiFen; Chiu, Shang-Yi; Chang, Chawnshang; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5083 - 5090
