in N,N,N',N',N'',N''-hexamethylphosphoric triamide Product distribution;

1: benzyl alcohol With trifluoromethylsulfonic anhydride; bis-(phenyl)-sulfoxide; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine in toluene T=-78°C; 1 h; 2: sodium acetophenoxide in tetrahydrofuran; toluene T=-78 - 20°C;

in tetrahydrofuran 12 h; -78 deg C -> r.t.; Yield given;

1: acetone-oxime With trifluoromethylsulfonic anhydride; triethylamine in toluene T=-78°C; 0.0833333 h; 2: sodium acetophenoxide in toluene T=-78 - 20°C; 1 h;

in N,N,N',N',N'',N''-hexamethylphosphoric triamide Product distribution;