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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
344453-19-6
合成路线
（共 10 条）
5798-75-4
4-溴苯甲酸乙酯
+
344453-19-6
→
反应条件
47230-38-6
联苯-4,4-草酸二乙酯
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
5798-75-4
4-溴苯甲酸乙酯
+
344453-19-6
→
反应条件
93-89-0
安息香酸乙酯
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
7206-23-7
+
111-66-0
1-辛烯
+
56318-80-0
反应条件
PEPPSI in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Organic Letters, , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
111-66-0
1-辛烯
+
56318-80-0
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Organic Letters, , vol. 13, # 15 p. 3818 - 3821
103-64-0
β-溴苯乙烯
+
344453-19-6
→
反应条件
117780-29-7
反应条件
mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
588-73-8
+
344453-19-6
→
反应条件
117780-29-7
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
56318-80-0
反应条件
trifuran-2-yl-phosphane; palladium dichloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
7206-23-7
+
111-66-0
1-辛烯
+
56318-80-0
反应条件
PEPPSI in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
7206-23-7
+
56318-80-0
反应条件
mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
344453-19-6
+
52356-93-1
→
反应条件
7206-35-1
+
111-66-0
1-辛烯
+
56318-80-0
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; Negishi coupling reaction; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Krasovskiy, Arkady; Lipshutz, Bruce H.
Organic Letters, 2011 , vol. 13, # 15 p. 3818 - 3821
