5-苯基二硫杂环戊烯-3-硫酮合成路线 （共 57 条）
反应条件
1H-imidazole; bis(trimethylsilyl)-sulfide in dichloromethane
18 h; Ambient temperature; Yield given;
参考文献
Curphey, Thomas J.; Joyner, H. Howard
Tetrahedron Letters, 1993 , vol. 34, # 45 p. 7231 - 7234
反应条件
1: 40 percent / ethanol / 0.17 h / Heating
2: 81 percent / benzene / 0.5 h / Heating
3: 13.9 percent / ethanol / 0.17 h / Heating
View Scheme
参考文献
Mitchell, James A.; Reid, David H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 499 - 507
反应条件
1: 78 percent / CH3OH, Na / tetrahydrofuran
2: 9 percent / decahydronaphthalene / 0.5 h / Heating
View Scheme
参考文献
Behringer, Hans; Meinetsberger, Eike
Liebigs Annalen der Chemie, 1981 , # 10 p. 1729 - 1750
参考文献
Boettcher; Luettringhaus
Justus Liebigs Annalen der Chemie, 1947 , vol. 557, p. 89,105
Full Text Show Details
Woronkow; Broun; Karpenko
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1927,1939
Chem.Abstr., 1950 , p. 1955
反应条件
trimethylamine-N-oxide in acetonitrile
under Ar; soln. of trimethylamine-N-oxide (5 equiv.) in MeCN added dropwise to MeCN soln. of Mo complex; heated at 65°C for 45 min;
参考文献
Mathur, Pradeep; Avasare, Vidya D.; Ghosh, Abhijit K.; Mobin, Shaikh M.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 7 p. 1325 - 1327
反应条件
trimethylamine-N-oxide in acetonitrile
under Ar; soln. of trimethylamine-N-oxide (5 equiv.) in MeCN added dropwise to MeCN soln. of Mo complex; heated at 65°C for 45 min;
参考文献
Mathur, Pradeep; Avasare, Vidya D.; Ghosh, Abhijit K.; Mobin, Shaikh M.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 7 p. 1325 - 1327
反应条件
diphosphorus pentasulfide
T=150°C;
参考文献
Tornetta
Annali di Chimica (Rome, Italy), 1958 , vol. 48, p. 577,580
反应条件
diphosphorus pentasulfide
T=150°C;
参考文献
Tornetta
Annali di Chimica (Rome, Italy), 1958 , vol. 48, p. 577,580
反应条件
diphosphorus pentasulfide
T=150°C;
参考文献
Tornetta
Annali di Chimica (Rome, Italy), 1958 , vol. 48, p. 577,580
反应条件
piperidine; hydrogen sulfide; diphosphorus pentasulfide; sulfur; xylene
T=130°C;
参考文献
Wander A.G.
Patent: DE909097 , 1951 ;
