对甲苯基[2-(三甲基甲硅烷基)乙炔基]砜合成路线 （共 8 条）
反应条件
aluminium trichloride in dichloromethane
参考文献
Otten, Albert; Namyslo, Jan Christoph; Stoermer, Martin; Kaufmann, Dieter E.
European Journal of Organic Chemistry, 1998 , # 9 p. 1997 - 2001
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 3 h; Ambient temperature;
参考文献
Back, Thomas G.; Collins, Scott; Kerr, Russell G.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3077 - 3084
反应条件
1: 94 percent / azobis(isobutyronitrile) / benzene / 96 h / 80 °C / sealed glass tube 2: 39 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Back, Thomas G.; Collins, Scott; Kerr, Russell G.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3077 - 3084
反应条件
1: 94 percent / azobis(isobutyronitrile) / benzene / 96 h / 80 °C / sealed glass tube 2: 39 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Back, Thomas G.; Collins, Scott; Kerr, Russell G.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3077 - 3084
反应条件
N-bromosuccinmide; silver nitrate in acetone T=20°C;
参考文献
Poulsen, Thomas B.; Bernardi, Luca; Aleman, Jose; Overgaard, Jacob; Jorgensen, Karl Anker
Journal of the American Chemical Society, 2007 , vol. 129, # 2 p. 441 - 449
反应条件
1: 79 percent / K2CO3, KHCO3 / H2O; methanol / 30 °C 2: 64 percent / 16 h / 80 °C View Scheme
参考文献
Dolci, Lilian; Dolle, Frederic; Valette, Heric; Vaufrey, Francoise; Fuseau, Chantal; Bottlaender, Michel; Crouzel, Christian
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 3 p. 467 - 479
反应条件
NAF in methanol; water T=10°C; 0.25 h;
参考文献
Otten, Albert; Namyslo, Jan Christoph; Stoermer, Martin; Kaufmann, Dieter E.
European Journal of Organic Chemistry, 1998 , # 9 p. 1997 - 2001
反应条件
2: 93 percent / Na-Hg, NaH2PO4*2H2O / methanol
View Scheme
参考文献
Davis, Anthony P.; Whitham, Gordon H.
Journal of the Chemical Society, Chemical Communications, 1980 , # 13 p. 639 - 640
