4-(甲基巯基)苯甲醛合成路线 (共 113 条)
反应条件
indium; tungsten hexachloride in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Yoo, Byung Woo; Kim, Hyung Min; Kim, Ducki; Seok, Kyoung Sun
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 8 p. 2525 - 2526
反应条件
Co(NO3)2⋅6H2O; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; Mn(NO3)2*4H2O; oxygen; acetic acid T=40°C; P=760.051 Torr; 0.75 h;
参考文献
Chinnusamy, Tamilselvi; Reiser, Oliver
ChemSusChem, 2010 , vol. 3, # 9 p. 1040 - 1042
反应条件
copper(l) iodide; ZnF2 T=150°C; 36 h; Sealed tubeUnder air;
参考文献
Luo, Fang; Pan, Changduo; Li, Liping; Chen, Fan; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 18 p. 5304 - 5306
反应条件
N,N,N',N,-tetramethylethylenediamine; hydrogen; palladium diacetate; propyl di-tert-butylphosphinite in toluene T=100°C; P=3750.38 Torr; 20 h; Inert atmosphere;
参考文献
Neumann, Helfried; Kadyrov, Renat; Wu, Xiao-Feng; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 10 p. 2213 - 2216
反应条件
copper(l) iodide; oxygen in dimethyl sulfoxide T=120°C; 25 h; chemoselective reaction;
参考文献
Zhang, Lin; Bi, Xihe; Guan, Xiaoxue; Li, Xingqi; Liu, Qun; Barry, Badru-Deen; Liao, Peiqiu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11303 - 11307
Angew. Chem., 2013 , vol. 125, # 43 p. 11513 - 11517,5
反应条件
2,6-bis-{[(E)-2,3,4-trifluoro-phenylimino]-methyl}-pyridine; zinc; nickel dichloride in N,N-dimethyl-formamide T=160°C; 24 h;
参考文献
Baldovino-Pantaleon, Oscar; Hernandez-Ortega, Simon; Morales-Morales, David
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 1-2 p. 236 - 242
反应条件
polystyrene-supported hypervalent iodine(V) reagent in 1,2-dichloro-ethane T=85°C; 1 h;
参考文献
Organic Letters, , vol. 8, # 1 p. 167 - 170
反应条件
1-iodyl-2-butoxybenzene in acetonitrile 15 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 71, # 22 p. 8452 - 8458
反应条件
dihydrogen peroxide T=70°C; 1 h;
参考文献
Shi, Feng; Tse, Man Kin; Kaiser, Hanns Martin; Beller, Matthias
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 16 p. 2425 - 2430
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Hass-Bender/Henry reaction;
参考文献
Klein, Thomas A.; Schkeryantz, Jeffrey M.
Tetrahedron Letters, 2005 , vol. 46, # 27 p. 4535 - 4538