4-(甲基巯基)苯甲醛合成路线 （共 113 条）
反应条件
1: 5.5 g / H2O2 / 2,2,2-trifluoro-ethanol; CH2Cl2; H2O / 4 h / 20 °C
2: 2,6-lutidine / various solvent(s) / 0.5 h / 20 °C
3: 5.73 g / TEA / methanol / 4 h / 20 °C
View Scheme
参考文献
Erlandsson, Mikael; Unden, Anders
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5829 - 5832
反应条件
1: pyridine; piperidine
2: H2O2; acetic acid
View Scheme
参考文献
Dani; Nargund
Journal of the Karnatak University, 1959 , vol. 4, p. 26,28
反应条件
tetra-(n-butyl)ammonium iodide in water
T=40°C; 24 h;
参考文献
Wei, Wei; Zhang, Chao; Xu, Yuan; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 38 p. 10827 - 10829
反应条件
1: 89 percent / 1percent aq. NaOH / 3 h / Ambient temperature
2: 54 percent / m-chloroperbenzoic acid / CHCl3 / 0.5 h / -15 °C
View Scheme
参考文献
Sulko, Jerzy
Acta Poloniae Pharmaceutica - Drug Research, 1998 , vol. 55, # 5 p. 403 - 411
反应条件
1: 80 percent / aq. NaOH / 24 h / Ambient temperature
2: 65 percent / aq. Et3N / 8 h / Heating
3: 90 percent / aq. H2O2, H2SO4 / Ambient temperature
View Scheme
参考文献
Rehse; Ruther
Archiv der Pharmazie, 1984 , vol. 317, # 2 p. 163 - 167
反应条件
[Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; hydroxylamine hydrochloride; sodium hydrogencarbonate in water
T=100°C; 7 h; Inert atmosphereSealed tubeGreen chemistry;
参考文献
Garcia-Alvarez, Rocio; Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
RSC Advances, 2013 , vol. 3, # 17 p. 5889 - 5894
反应条件
tert.-butylhydroperoxide; sodium hydroxide; (CTA)2SO4
T=50°C; 2 h;
参考文献
Fringuelli; Pellegrino; Piermatti; Pizzo
Synthetic Communications, 1994 , vol. 24, # 18 p. 2665 - 2673
参考文献
Rehse; Ruther
Archiv der Pharmazie, 1984 , vol. 317, # 3 p. 262 - 267
反应条件
Yield given. Multistep reaction;
参考文献
Najib, Jamila; Caumont-Bertrand, Karine
Patent: US2005/176808 A1, 2005 ;
Location in patent: Page/Page column 17 ;
反应条件
1: zinc iodide / neat (no solvent) / 0.25 h
2: ammonia / methanol / 2 h / 40 °C
View Scheme
参考文献
Mai; Patil
Tetrahedron Letters, 1984 , vol. 25, # 41 p. 4583 - 4586
