4-(甲基巯基)苯甲醛合成路线 (共 113 条)
反应条件
1: sodium sulfide / das Natriumsalz entsteht 2: alkali View Scheme
参考文献
Chemische Berichte, , vol. 45, p. 2087
参考文献
Chemische Berichte, , vol. 45, p. 2087
反应条件
in toluene 0.5 h; UV-irradiation; Product distribution; Further Variations:title compound concentration; light intensity;
参考文献
Journal of Organic Chemistry, , vol. 72, # 8 p. 2757 - 2768
反应条件
N-methyl-N,N-di(2-hydroxyethyl)amine Irradiation; KineticsMechanismQuantum yield; Reagent/catalyst;
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 51, # 8 p. 1865 - 1871
反应条件
tert.-butylhydroperoxide; sodium hydroxide T=70°C; 2 h;
参考文献
Fringuelli; Pellegrino; Piermatti; Pizzo
Synthetic Communications, 1994 , vol. 24, # 18 p. 2665 - 2673
反应条件
sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide in water; acetonitrile T=10°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Dalcanale, Enrico; Montanari, Fernando
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 567 - 569
反应条件
hydrogen; 12-phosphotungstic acid; [Fe(C5H4P(i-Pr)2)2Rh(C8H12)]BF4 in water; isopropyl alcohol T=20°C; P=5171.62 Torr; 16 h;
参考文献
Vu, Thi-Thu-Ha; Kumbhar, Pramod S.; Figueras, Francois
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 4 p. 493 - 496
反应条件
sodium tetrahydroborate; nickel dichloride in methanol 18 h; Ambient temperature;
参考文献
Euerby, Melvin R.; Waigh, Roger D.
Synthetic Communications, 1986 , vol. 16, # 7 p. 779 - 784
反应条件
acetic anhydride; triethylamine in water
参考文献
G. D. Searle and Co.
Patent: US5859257 A1, 1999 ;
反应条件
sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide in water; acetonitrile T=10°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Dalcanale, Enrico; Montanari, Fernando
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 567 - 569