4-(甲基巯基)苯甲醛合成路线 （共 113 条）
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
反应条件
piperidine in toluene 0.5 h; Heating;
参考文献
Bogeso
Journal of Medicinal Chemistry, 1983 , vol. 26, # 7 p. 935 - 947
反应条件
graphite; potassium bromide in water T=25°C; Electrolysis;
参考文献
De Souza, Carlos A.; Navarro, Marcelo; Bieber, Lothar W.; Areias, Madalena C.C.
Electrochimica Acta, 2014 , vol. 132, p. 118 - 126
反应条件
1: MeSNa / hexamethylphosphoric acid triamide / 18 h / 100 °C 2: 1.05 g / hexamethylphosphoric acid triamide / 2 h View Scheme
参考文献
Gryko, Daniel T.; Clausen, Christian; Lindsey, Jonathan S.
Journal of Organic Chemistry, 1999 , vol. 64, # 23 p. 8635 - 8647
反应条件
1: pyridine; piperidine 2: H2O2; acetic acid View Scheme
参考文献
Dani; Nargund
Journal of the Karnatak University, 1959 , vol. 4, p. 26,28
反应条件
sodium hydroxide; 3-chloro-benzenecarboperoxoic acid T=1 - 3°C; 2 h;
参考文献
Fringuelli; Pellegrino; Piermatti; Pizzo
Synthetic Communications, 1994 , vol. 24, # 18 p. 2665 - 2673
反应条件
sodium dithionite in formic acid; toluene
参考文献
Societe Anonyme dite: L'Oreal
Patent: US4980509 A1, 1990 ;
反应条件
dihydrogen peroxide T=50°C; 4 h;
参考文献
Synlett, , # 12 p. 2031 - 2034
Tetrahedron, , vol. 60, # 18 p. 4087 - 4096
反应条件
in 1-methyl-pyrrolidin-2-one T=100°C; 14 h;
参考文献
Lu, Xingliang; Rodriguez, Maria; Gu, Wenxin; Silverman, Richard B.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 20 p. 4423 - 4430
反应条件
potassium tert-butylate; toluene-4-sulfonic acid in methanol T=20°C; 1.5 h; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 2, # 1 p. 10 - 17
