carbon tetrabromide; triphenylphosphine in dichloromethane T=0°C; 0.666667 h;
参考文献
Ivanov, I. V.; Groza, N. V.; Mnasina, E. E.; Myagkova, G. I.
Russian Journal of Bioorganic Chemistry, 1995 , vol. 21, # 10 p. 696 - 699
Bioorganicheskaya Khimiya, 1995 , vol. 21, # 10 p. 802 - 805
1: K2CO3, NaI, CuI / dimethylformamide / 4 h / 20 °C 2: K2CO3 / methanol / 4 h / 20 °C 3: 81.9 percent / PPh3, CBr4 / CH2Cl2 / 0.67 h / 0 °C 4: K2CO3, NaI, CuI / dimethylformamide / 5 h / 20 °C 5: p-toluenesulfonic acid / methanol / 1 h / 20 °C 6: 79.2 percent / PPh3, CBr4 / CH2Cl2 / 0.67 h / 0 °C View Scheme
参考文献
Ivanov, I. V.; Groza, N. V.; Mnasina, E. E.; Myagkova, G. I.
Russian Journal of Bioorganic Chemistry, 1995 , vol. 21, # 10 p. 696 - 699
Bioorganicheskaya Khimiya, 1995 , vol. 21, # 10 p. 802 - 805
1: 0.89 g / K2CO3, NaI, CuI / dimethylformamide / 5 h / 20 °C 2: 66.3 percent / 5percent aq. NaOH / methanol / 3 h / 20 °C 3: 1.) H2, quinoline, 2.) H2O / 1.) Lindlar's cat. / 1.) AcOEt View Scheme
参考文献
Ivanov, I. V.; Groza, N. V.; Mnasina, E. E.; Myagkova, G. I.
Russian Journal of Bioorganic Chemistry, 1995 , vol. 21, # 10 p. 696 - 699
Bioorganicheskaya Khimiya, 1995 , vol. 21, # 10 p. 802 - 805
