4,4'-二氟二苯甲酮合成路线 (共 115 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=60°C; 4 h;
参考文献
Rao, Maddali L. N.; Venkatesh, Varadhachari; Dasgupta, Priyabrata
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 4975 - 4980
反应条件
potassium phosphate; palladium diacetate T=20°C; 3 h;
参考文献
Zhou, Qing; Wei, Shaohua; Han, Wei
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1454 - 1460
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=60°C; P=30002.4 Torr; 18 h;
参考文献
Chemical Communications, , # 13 p. 1520 - 1521
反应条件
Ru(bpy)3Cl2; caesium carbonate in N,N-dimethyl acetamide T=25°C; 48 h; Irradiation;
参考文献
Su, Yijin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2011 , vol. 13, # 9 p. 2168 - 2171
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; triphenylphosphine in benzene T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 7 p. 2161 - 2163
反应条件
in o-di-fluorobenzene; 1,2-dichloro-benzene
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 4 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 38 p. 4975 - 4980
反应条件
N,N-dimethyl acetamide; tetramethyl-ammonium fluoride T=100°C; 1 h;
参考文献
Adams, Dave J.; Clark, James H.; McFarland, Heather
Journal of Fluorine Chemistry, 1998 , vol. 92, # 2 p. 127 - 129
反应条件
[bmim][NTf2]2; zinc(II) chloride T=160°C; Friedel-Crafts reaction; P=3750.3 Torr; 18 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 12 p. 1368 - 1369
反应条件
chromium(VI) oxide; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 69, p. 662
Rev. Inst. SalubridadChem.Abstr., , vol. 8, p. 63,66
Rev. Inst. SalubridadChem.Abstr., , p. 1920