4,4'-二氟二苯甲酮合成路线 （共 115 条）
反应条件
carbon disulfide; aluminium trichloride 3-taegiges Behandeln des Reaktionsprodukts mit konz. Schwefelsaeure;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 135, p. 245,252
反应条件
aluminium trichloride
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 7, p. 71,82
反应条件
copper(II) nitrate in dichloromethane 1 h; Mechanism;
参考文献
Chemistry Letters, , p. 1187 - 1190
反应条件
gallium trifluoromethanesulfonate; dimethylmono-chlorosilane in dichloromethane T=20°C; 1.5 h;
参考文献
Surya Prakash; Do, Clement; Mathew, Thomas; Olah, George A.
Catalysis Letters, 2011 , vol. 141, # 4 p. 507 - 511
反应条件
potassium hydroxide; oxygen in ethylene glycol dimethyl ether T=70°C; 3 h;
参考文献
Artamkina, G. A.; Grinfel'd, A. A.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 345 - 352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 383 - 391
参考文献
Journal of Chemical Research - Part S, , # 2 p. 69 - 71
反应条件
potassium hydroxide; oxygen in ethylene glycol dimethyl ether T=70°C; 3 h;
参考文献
Artamkina, G. A.; Grinfel'd, A. A.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 345 - 352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 383 - 391
反应条件
in tetrahydrofuran 2 h; Heating;
参考文献
Dhar; Borden; Tyagarajan; Smith; Branchek; Weinshank; Gluchowski
Journal of Medicinal Chemistry, 1994 , vol. 37, # 15 p. 2334 - 2342
反应条件
magnesium 1.) terbutyl methyl ether, THF, iodine, dichloroethane, reflux, 2.) reflux, 2.5 h; Multistep reaction;
参考文献
Bartroli; Alguero; Boncompte; Forn
Arzneimittel-Forschung/Drug Research, 1992 , vol. 42, # 6 p. 832 - 835
反应条件
1.1: NaH / toluene / 0.5 h / 4 °C 1.2: 69 percent / toluene / 20 °C 2.1: 98 percent / DibAl-H / toluene / 1 h / -5 - 20 °C View Scheme
参考文献
Pinna, Gerard Aime; Cignarella, Giorgio; Ruiu, Stefania; Loriga, Giovanni; Murineddu, Gabriele; Villa, Stefania; Grella, Giuseppe Enrico; Cossu, Gregorio; Fratta, Walter
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4015 - 4026
