(2-氧代-2-苯乙基)膦酸二乙酯合成路线 （共 61 条）
反应条件
1: 80 percent / t-BuOK / dimethylsulfoxide / 0.08 h / 25 °C 2: 78 percent Chromat. / t-BuOK / dimethylsulfoxide / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 8 p. 1836 - 1842
参考文献
Chemistry Letters, , p. 831 - 834
反应条件
in dimethyl sulfoxide 8 h; Irradiation; Yield given;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
triethylamine; magnesium chloride in acetonitrile Acylation; 2 h; Heating;
参考文献
Synthetic Communications, , vol. 30, # 4 p. 609 - 618
反应条件
1: toluene / 3 h / Heating 2: 90 percent / acetone, aq. hydrochloric acid / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 11 p. 1048 - 1051
反应条件
1: 3 h / Ambient temperature 2: toluene / 3 h / Heating 3: 90 percent / acetone, aq. hydrochloric acid / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 11 p. 1048 - 1051
反应条件
1: Et3N / toluene / 1 h / Ambient temperature 2: MgCl2 / toluene / 12 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 1360 - 1364
反应条件
1: 1.) THF, RT, 1 h, 2.) THF, RT, 2 h 2: aq. NaOCl / CHCl3 / 0.5 h / Ambient temperature View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 90, # 1-4 p. 47 - 52
反应条件
1: (i) PCl5, benzene, (ii) SO2 2: Et3N / diethyl ether 3: aq. HCl View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 604 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 675 - 683
反应条件
1: quinoline, (1S)-2-oxo-bornane-10-sulfonic acid 2: (i) PCl5, benzene, (ii) SO2 3: Et3N / diethyl ether 4: aq. HCl View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 604 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 675 - 683
