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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3453-63-2
合成路线
（共 40 条）
577-56-0
2-乙酰苯甲酸
→
反应条件
3453-63-2
反应条件
N,N,N',N'-tetramethyl-O-(N-succinimidyl)uronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 6 h; Inert atmosphere; TemperatureReagent/catalyst;
参考文献
He, Xinhua; Xue, Fengtian
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1956 - 1958
33578-00-6
2-乙炔苯甲酸
→
反应条件
3453-63-2
反应条件
in N-butylamine T=90°C; 36 h;
参考文献
Varela-Fernandez, Alejandro; Gonzalez-Rodriguez, Carlos; Varela, Jesus A.; Castedo, Luis; Saa, Carlos
Organic Letters, 2009 , vol. 11, # 22 p. 5350 - 5353
1066-54-2
三甲基乙炔基硅
+
88-65-3
邻溴苯甲酸
→
反应条件
3453-63-2
反应条件
1: 2-Bromobenzoic acid With copper(l) iodide; palladium 10 on activated carbon; triethylamine; triphenylphosphine in 1,4-dioxane T=25°C; 0.5 h; Inert atmosphere; 2: trimethylsilylacetylene in 1,4-dioxane T=80°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Rambabu; Kumar, G. Pavan; Kumar, Barange Deepak; Kapavarapu, Ravikumar; Rao, M.V. Basaveswara; Pal, Manojit
Tetrahedron Letters, 2013 , vol. 54, # 23 p. 2989 - 2995
33578-00-6
2-乙炔苯甲酸
→
反应条件
491-31-6
异薰草素
+
3453-63-2
反应条件
potassium carbonate; gold(I) chloride in acetonitrile T=20°C; 2 h;
参考文献
Marchal, Estelle; Uriac, Philippe; Legouin, Beatrice; Toupet, Loic; Weghe, Pierre van de
Tetrahedron, 2007 , vol. 63, # 40 p. 9979 - 9990
201230-82-2
+
129849-05-4
→
反应条件
3453-63-2
反应条件
triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide T=60°C; 1 h;
参考文献
Ciattini; Mastropietro; Morera; Ortar
Tetrahedron Letters, 1993 , vol. 34, # 23 p. 3763 - 3766
88-67-5
邻碘苯甲酸
+
74-86-2
乙炔
→
反应条件
3453-63-2
反应条件
triethylamine; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=60°C;
参考文献
Liao, Hong-Yueh; Cheng, Chien-Hong
Journal of Organic Chemistry, 1995 , vol. 60, # 12 p. 3711 - 3716
38846-64-9
2-乙炔基苯甲醛
→
反应条件
3453-63-2
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in tetrahydrofuran; water; tert-butyl alcohol T=0 - 70°C; 14 h; regioselective reaction;
参考文献
Li, Jim; Chin, Elbert; Lui, Alfred S.; Chen, Lijing
Tetrahedron Letters, 2010 , vol. 51, # 45 p. 5937 - 5939
953395-26-1
→
反应条件
反应条件
mercury(II) trifluoromethanesulfonate in dichloromethane T=25°C; 2 h;
参考文献
Yamamoto, Hirofumi; Pandey, Ghanshyam; Asai, Yumiko; Nakano, Mayo; Kinoshita, Atsushi; Namba, Kosuke; Imagawa, Hiroshi; Nishizawa, Mugio
Organic Letters, 2007 , vol. 9, # 20 p. 4029 - 4032
129849-05-4
+
12539-63-8
→
反应条件
3453-63-2
反应条件
1,3-bis-(diphenylphosphino)propane; palladium diacetate; triethylamine in N,N-dimethyl-formamide T=60°C;
参考文献
Ortar, Giorgio; Schiano Moriello, Aniello; Morera, Enrico; Nalli, Marianna; Di Marzo, Vincenzo; De Petrocellis, Luciano
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 20 p. 5614 - 5618
550365-39-4
→
反应条件
3453-63-2
反应条件
formic acid; triethylamine; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=60 - 63°C; 30 h;
参考文献
Rossi, Renzo; Carpita, Adriano; Bellina, Fabio; Stabile, Paolo; Mannina, Luisa
Tetrahedron, 2003 , vol. 59, # 12 p. 2067 - 2081
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