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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
34535-98-3
合成路线
（共 12 条）
400777-68-6
→
反应条件
34535-98-3
反应条件
hydrogen; palladium on activated charcoal in methanol; acetic acid P=3000.3 Torr; 4 h;
参考文献
Wimalasena, Kandatege; Wickman, Heang B.; Mahindaratne, Mathew P. D.
European Journal of Organic Chemistry, 2001 , # 20 p. 3811 - 3817
108-86-1
溴代苯
+
765-30-0
环丙胺
→
反应条件
34535-98-3
反应条件
tris-(dibenzylideneacetone)dipalladium(0); sodium tert-pentoxide; (R)-p-tol-BINAP in toluene T=80°C; 18 h; Inert atmosphere;
参考文献
Maity, Soumitra; Zhu, Mingzhao; Shinabery, Ryan Spencer; Zheng, Nan
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 222 - 226
321532-64-3
→
反应条件
34535-98-3
反应条件
potassium hydroxide in 1-methyl-pyrrolidin-2-one; toluene T=120 - 130°C; Smiles Aromatic Rearrangement;
参考文献
Arava, Veera Reddy; Bandatmakuru, Sreenivasula Reddy
Synthesis (Germany), 2013 , vol. 45, # 8 art. no. SS-2013-Z0041-OP, p. 1039 - 1044
603-33-8
三苯基铋
+
765-30-0
环丙胺
→
反应条件
34535-98-3
反应条件
copper diacetate in dichloromethane T=20°C; 18 h;
参考文献
Bishop, Michael J.; Garrido, Dulce M.; Boswell, G. Evan; Collins, Mark A.; Harris, Philip A.; McNutt, Robert W.; O'Neill, Scott J.; Wei, Ke; Chang, Kwen-Jen
Journal of Medicinal Chemistry, 2003 , vol. 46, # 4 p. 623 - 633
16350-99-5
→
反应条件
34535-98-3
反应条件
1: 80 percent / Ti(OiPr)4 / tetrahydrofuran / 24 h 2: 62 percent / H2 / Pd/C / methanol; acetic acid / 4 h / 3000.3 Torr View Scheme
参考文献
Wimalasena, Kandatege; Wickman, Heang B.; Mahindaratne, Mathew P. D.
European Journal of Organic Chemistry, 2001 , # 20 p. 3811 - 3817
103-70-8
N-苯基甲酰胺
→
反应条件
34535-98-3
反应条件
1: 50 percent / K2CO3 / dimethylsulfoxide; tetrahydrofuran / 72 h / Heating 2: 80 percent / Ti(OiPr)4 / tetrahydrofuran / 24 h 3: 62 percent / H2 / Pd/C / methanol; acetic acid / 4 h / 3000.3 Torr View Scheme
参考文献
Wimalasena, Kandatege; Wickman, Heang B.; Mahindaratne, Mathew P. D.
European Journal of Organic Chemistry, 2001 , # 20 p. 3811 - 3817
→
反应条件
34535-98-3
反应条件
1: With methanol; acetic acid T=67 - 69°C; 5 h; 2: With sodium tetrahydroborate; boron trifluoride-tetrahydrofuran complex in tetrahydrofuran T=60°C; 4 h;
参考文献
Yoshida, Yasuo; Umezu, Kazuto; Hamada, Yusuke; Atsumi, Naoya; Tabuchi, Fumiya
Synlett, 2003 , # 14 p. 2139 - 2142
725242-37-5
→
反应条件
74497-02-2
+
34535-98-3
反应条件
potassium phosphate buffer; dihydrogen peroxide; horseradish peroxidase in acetonitrile T=20°C; pH=5.5; Enzyme kinetics;
参考文献
Totah; Hanzlik
Journal of the American Chemical Society, 2001 , vol. 123, # 41 p. 10107 - 10108
→
反应条件
34535-98-3
反应条件
3 Angstroem MS; sodium cyanoborohydride in methanol; acetic acid 16 h; Heating;
参考文献
Gillaspy, Melissa L.; Lefker, Bruce A.; Hada, William A.; Hoover, Dennis J.
Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7399 - 7402
74497-02-2
→
反应条件
34535-98-3
反应条件
1: 83 percent / Et3N / CH2Cl2 / 29 h / Heating 2: 1) NaBH4, BF4*OEt2 / 1) THF, 0 deg C, 0.5 h; 2) THF, 1 h, 0 deg C View Scheme
参考文献
Blackburn, Anthony; Bowles, Daniel M.; Curran, Timothy T.; Kim, Hui
Synthetic Communications, 2012 , vol. 42, # 12 p. 1855 - 1863
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